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All 2 posts Subject: microwave safrole isomerization Please login to post Down

maxscorpio
(Stranger)
09-09-03 11:18
No 457894
microwave safrole isomerization

anybody tried a microwave for this. other than the huge amount of koh used, any drawbacks or problems for this method. i UTFSE, but came up with zero results strangely, are there any writeups other than rhodiums.
This method sounds so quick with great yields.

Rhodium
(Chief Bee)
09-09-03 15:53
No 457915
User Picture Microwave Isomerization of Allylbenzenes

Nothing in TFSE? A simple search for "isomerization microwave" gave among other things the following excellent threads:

Post 291995 (foxy2: "Safrole Isomerization in microwave", Chemistry Discourse)
Post 108400 (dormouse: "Microwave Isomerization of Safrole - Cherrie Baby", Novel Discourse)
Post 162640 (jimwig: "microwaves for honey", Methods Discourse)

latest addition (09-09-03): Edit: New addition to my page:

Isomerization Of Safrole And Eugenol Under Microwave Irradiation
G. V. Salmoria, E. L. Dall'Oglio, C. Zucco
Synthetic Communications, 27(24), 4335-4340 (1997) (https://www.rhodium.ws/chemistry/isomerizafrole.mw-0.html)

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	All 2 posts		Subject: microwave safrole isomerization		Please login to post		Down


		maxscorpio (Stranger) 09-09-03 11:18 No 457894				microwave safrole isomerization
						anybody tried a microwave for this. other than the huge amount of koh used, any drawbacks or problems for this method. i UTFSE, but came up with zero results strangely, are there any writeups other than rhodiums. This method sounds so quick with great yields.



		Rhodium (Chief Bee) 09-09-03 15:53 No 457915				Microwave Isomerization of Allylbenzenes
						Nothing in TFSE? A simple search for "isomerization microwave" gave among other things the following excellent threads: Post 291995 (foxy2: "Safrole Isomerization in microwave", Chemistry Discourse) Post 108400 (dormouse: "Microwave Isomerization of Safrole - Cherrie Baby", Novel Discourse) Post 162640 (jimwig: "microwaves for honey", Methods Discourse) (09-09-03): Edit: New addition to my page: Isomerization Of Safrole And Eugenol Under Microwave Irradiation G. V. Salmoria, E. L. Dall'Oglio, C. Zucco Synthetic Communications, 27(24), 4335-4340 (1997) (https://www.rhodium.ws/chemistry/isomerizafrole.mw-0.html)

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