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All 8 posts Subject: a-thujone Please login to post Down

eXcidium
(Newbee)
05-05-04 06:05
No 504962
      a-thujone

Hi

Does anyone have idea if this substances (alpha-thujone or beta-thujone) have a synthesis published somewhere?

Thanks

"Ipsa scientia potestas est."

hest
(Hive Adickt)
05-05-04 09:27
No 504985
      Thujone

It's made in the nature, you can by it for almost free. And I'm sure that the total synthesis i loooong and hard to come over.

eXcidium
(Newbee)
05-05-04 23:23
No 505133
      here

Hey hest - and thanks

Well buy it for almost free.. tthat would be good
Wormwood oil - 99% thujone (1L) = $300
I wouldn't call that cheap :p

The synthesis would be a best way, i think

"Ipsa scientia potestas est."

Aurelius
(Active Asperger Archivist)
05-06-04 02:12
No 505171
      Synthesis

synthesis of thujone vs its purchase at $300.00/L ......

buy the stuff- saves time, MONEY, effort, requires no chemicals, labs, glassware, etc.

are you familiar with synthesis at all?

Act quickly or not at all.

eXcidium
(Newbee)
05-06-04 02:20
No 505175
User Picture       Indeed

Indeed i am.

I have a nice lab setup (wich i bought in my college days), and have been boughting new stuff

Also reagents or no problem since chemistry (more like genetics/biochemistry) is my area

Glad if you could supply a synthesis of the said subtance

Cheers

"Ipsa scientia potestas est."

Rhodium
(Chief Bee)
05-06-04 04:20
No 505215
User Picture       Thujone

As late as 1981, thujone was preferentially isolated from natural oils over synthesis... It is not especially easy to synthesize a molecule consisting of a cyclopentane-cyclopropane bicycle with two chiral alkyl groups.

Solution-phase photodecarbonylation of the bicyclo[3.1.0]hexan-3-one system
Robert S. Cooke, Gregory D. Lyon
J. Am. Chem. Soc. 103, 7317-7322 (1981)

^{The Hive - Clandestine Chemists Without Borders}

eXcidium
(Newbee)
05-06-04 04:25
No 505217
User Picture       thx

Thanks Rhodium.. i'll check this out

"Ipsa scientia potestas est."

hest
(Hive Adickt)
05-06-04 09:17
No 505255
      These gay's make it from scrat's.

These gay's make it from scrat's. 300$/L is free trust mee.
But Iff you synt. it from bottom Il doo will respect you werye much.

http://journal.library.iisc.ernet.in/archives/V22.html

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		eXcidium (Newbee) 05-05-04 06:05 No 504962				a-thujone
						Hi Does anyone have idea if this substances (alpha-thujone or beta-thujone) have a synthesis published somewhere? Thanks "Ipsa scientia potestas est."



		hest (Hive Adickt) 05-05-04 09:27 No 504985				Thujone
						It's made in the nature, you can by it for almost free. And I'm sure that the total synthesis i loooong and hard to come over.



		eXcidium (Newbee) 05-05-04 23:23 No 505133				here
						Hey hest - and thanks Well buy it for almost free.. tthat would be good Wormwood oil - 99% thujone (1L) = $300 I wouldn't call that cheap :p The synthesis would be a best way, i think "Ipsa scientia potestas est."



		Aurelius (Active Asperger Archivist) 05-06-04 02:12 No 505171				Synthesis
						synthesis of thujone vs its purchase at $300.00/L ...... buy the stuff- saves time, MONEY, effort, requires no chemicals, labs, glassware, etc. are you familiar with synthesis at all? Act quickly or not at all.



		eXcidium (Newbee) 05-06-04 02:20 No 505175				Indeed
						Indeed i am. I have a nice lab setup (wich i bought in my college days), and have been boughting new stuff Also reagents or no problem since chemistry (more like genetics/biochemistry) is my area Glad if you could supply a synthesis of the said subtance Cheers "Ipsa scientia potestas est."



		Rhodium (Chief Bee) 05-06-04 04:20 No 505215				Thujone
						As late as 1981, thujone was preferentially isolated from natural oils over synthesis... It is not especially easy to synthesize a molecule consisting of a cyclopentane-cyclopropane bicycle with two chiral alkyl groups. Solution-phase photodecarbonylation of the bicyclo[3.1.0]hexan-3-one system Robert S. Cooke, Gregory D. Lyon J. Am. Chem. Soc. 103, 7317-7322 (1981) ^{The Hive - Clandestine Chemists Without Borders}



		eXcidium (Newbee) 05-06-04 04:25 No 505217				thx
						Thanks Rhodium.. i'll check this out "Ipsa scientia potestas est."



		hest (Hive Adickt) 05-06-04 09:17 No 505255				These gay's make it from scrat's.
						These gay's make it from scrat's. 300$/L is free trust mee. But Iff you synt. it from bottom Il doo will respect you werye much. http://journal.library.iisc.ernet.in/archives/V22.html

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