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Digest: PCP and Relatives: A Synthetic View Please login to post

Aurelius
(Active Asperger Archivist)
05-13-04 04:50
No 506789
PCP and Relatives: A Synthetic View
(Rated as: excellent)

Bear with me, this is a completely new project and I've got hundreds of links to put in. I'm very busy and this might take a few weeks or longer- but it's a popular enough topic that I thought it would be worth it.

PCPstraight-up

https://www.rhodium.ws/chemistry/pcp.shulgin.html
https://www.rhodium.ws/chemistry/pcp/cn_synth.html
Post 288137 (Antoncho: "A cool PCP synthesis", Novel Discourse)

Ideas on PCP Synthesis:
Post 475464 (ning: "phencyclidine sans cyclohexanone", Novel Discourse)

Analogues:

PCPy: Pyrrolidene analogue:
Post 101681 (The Alchemist: "Dust for the masses...", Chemistry Discourse) (read the whole thread)

4-MeO-PCP

https://www.rhodium.ws/chemistry/4-meo-pcp.html

Fluorinated Analogues:
Post 471106 (Rhodium: "Fluorinated PCP Analogs", Methods Discourse)

Contaminants:
Post 382798 (Rhodium: "PCP byproducts", Methods Discourse)
https://www.rhodium.ws/chemistry/pcp.pcc.analysis.html
Post 406851 (Rhodium: "Measuring PCC contamination of PCP", Methods Discourse) (same as above page)
Post 502110 (Rhodium: "Pyrolytic Fate of the PCP contaminant PCC", Methods Discourse)

TCP

Post 484668 (Xicori: "TCP Synthesis", Methods Discourse)
Bioassays
Post 486907 (Xicori: "Bioassay", Methods Discourse)

Contamination
PCC Detection
https://www.rhodium.ws/chemistry/pcp.pcc.analysis.html

PCDE

Synth and Bioassay
Post 369598 (Antoncho: "Zealot: synthesis and bioevaluation of PCDE", Novel Discourse)

PCM

Post 475049 (Xicori: "PCM synthesis", Methods Discourse)
Bioassay
Post 475116 (Xicori: "thanks for the flowers :-D details on bioassay", Methods Discourse)

Ketamine

https://www.rhodium.ws/chemistry/ketamine.html
https://www.rhodium.ws/chemistry/ketamine2.html

analogues:
Post 465673 (Manichi: "Discussion on possible ketamine analogs", Novel Discourse)
Post 505521 (ning: "Modified ketamine method", Novel Discourse)

Refs:If the refs aren't here in this digest or elsewhere at the Hive (so do a search), they would be appreciated.
Post 466915 (Manichi: "Ketamine References Feeding", Novel Discourse)
Post 466993 (Rhodium: "Ketamine Reference Feeding #2", Novel Discourse)

Tiletamine (SP?)

Eticylclidine
https://www.rhodium.ws/chemistry/eticyclidine.html

Rolicylidine
https://www.rhodium.ws/chemistry/eticyclidine.html

Others?

Please feel free to pm links, comments, suggestions etc. to Aurelius on this Digest or any others maintained by me.

MISC TO BE PLACED:
Post 455365 (Bwiti: "Novel Phenylcyclohexylamines..", Methods Discourse)
Post 424992 (Bwiti: "1-(1-Phenylcyclohexyl)-4-phenylpiperidine", Methods Discourse)

Patents:
contributed by Cyrax in:
Post 356567 (Cyrax: "PCP Patents, a compendium", Methods Discourse)
Patent GB836083
Patent GB837747
Patent US2921076
Patent US3097136
Patent US3145229
Patent US5248686

Contributed by Bwiti in:
Post 357544 (Bwiti: "That's good news!", Methods Discourse)
Patent GB758143
Patent GB838748
Patent GB853775
Patent GB861350
Patent US3192219
Patent US3097207
Patent GB836083
Patent GB837747
Patent US5969159
Patent US3097136
Patent US3145229
Patent US3097136
Patent US3247200
Patent US3522273
Patent US2921076
Patent US3254124

References Requested Specifically for this Digest:
Post 361229 (Bwiti: "Needed References", Methods Discourse)
(before sending of these refs- be sure that they haven't already been posted here or in posts subsequent to 361229 in that same thread)

Post 361271 (Rhodium: "More PCP", Methods Discourse)
Post 378784 (Rhodium: "Rigid PCP Analogs - Binding to Sigma/PCP receptors", Methods Discourse)

Mostly Pharm info, but some synth:
Post 507205 (7is: "More PCP related studies", Methods Discourse) -- be sure to check the following threads also.

Precursors
Cyclohexanone
by ox. of Cyclohexanol
with KMnO₄
Post 285993 (Elementary: "Oxidation of cyclohexanol with KMnO4", Methods Discourse)

1,5-Dibromopentane:
Post 436097 (pHarmacist: "1,5-dibromopentane", Methods Discourse)
Post 288137 (Antoncho: "A cool PCP synthesis", Novel Discourse)
Post 184706 (Rhodium: "Re: Help to make 1,5-dibromopentane (Method). for PCP", Novel Discourse)

PCA:
Post 105162 (Slappy: "PCA question", Chemistry Discourse)

PCC: 1-Piperidinyl Cyclohexanecarbonitrile (& analogues)
Post 172690 (slappy: "Re: Weight of PCC-Analogue(from methylamine).....", Chemistry Discourse)
Post 101408 (Beagle: "Question about 1-piperidine-carbonitrile...", Chemistry Discourse)

--

Post 465740 (josef_k: "phenylcyclopentylketone", Novel Discourse)
Post 465792 (Manichi: "Cyclohexene -persulfate/CuSO4->CyclopentaneCOOH", Novel Discourse)
Post 466155 (Vitus_Verdegast: "Great work Manichi!!", Novel Discourse)

Act quickly or not at all.

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			Digest: PCP and Relatives: A Synthetic View		Please login to post


		Aurelius (Active Asperger Archivist) 05-13-04 04:50 No 506789				PCP and Relatives: A Synthetic View (Rated as: excellent)
						Bear with me, this is a completely new project and I've got hundreds of links to put in. I'm very busy and this might take a few weeks or longer- but it's a popular enough topic that I thought it would be worth it. PCPstraight-up https://www.rhodium.ws/chemistry/pcp.shulgin.html https://www.rhodium.ws/chemistry/pcp/cn_synth.html Post 288137 (Antoncho: "A cool PCP synthesis", Novel Discourse) Ideas on PCP Synthesis: Post 475464 (ning: "phencyclidine sans cyclohexanone", Novel Discourse) Analogues: PCPy: Pyrrolidene analogue: Post 101681 (The Alchemist: "Dust for the masses...", Chemistry Discourse) (read the whole thread) 4-MeO-PCP https://www.rhodium.ws/chemistry/4-meo-pcp.html Fluorinated Analogues: Post 471106 (Rhodium: "Fluorinated PCP Analogs", Methods Discourse) Contaminants: Post 382798 (Rhodium: "PCP byproducts", Methods Discourse) https://www.rhodium.ws/chemistry/pcp.pcc.analysis.html Post 406851 (Rhodium: "Measuring PCC contamination of PCP", Methods Discourse) (same as above page) Post 502110 (Rhodium: "Pyrolytic Fate of the PCP contaminant PCC", Methods Discourse) TCP Post 484668 (Xicori: "TCP Synthesis", Methods Discourse) Bioassays Post 486907 (Xicori: "Bioassay", Methods Discourse) Contamination PCC Detection https://www.rhodium.ws/chemistry/pcp.pcc.analysis.html PCDE Synth and Bioassay Post 369598 (Antoncho: "Zealot: synthesis and bioevaluation of PCDE", Novel Discourse) PCM Post 475049 (Xicori: "PCM synthesis", Methods Discourse) Bioassay Post 475116 (Xicori: "thanks for the flowers :-D details on bioassay", Methods Discourse) Ketamine https://www.rhodium.ws/chemistry/ketamine.html https://www.rhodium.ws/chemistry/ketamine2.html analogues: Post 465673 (Manichi: "Discussion on possible ketamine analogs", Novel Discourse) Post 505521 (ning: "Modified ketamine method", Novel Discourse) Refs:If the refs aren't here in this digest or elsewhere at the Hive (so do a search), they would be appreciated. Post 466915 (Manichi: "Ketamine References Feeding", Novel Discourse) Post 466993 (Rhodium: "Ketamine Reference Feeding #2", Novel Discourse) Tiletamine (SP?) Eticylclidine https://www.rhodium.ws/chemistry/eticyclidine.html Rolicylidine https://www.rhodium.ws/chemistry/eticyclidine.html Others? Please feel free to pm links, comments, suggestions etc. to Aurelius on this Digest or any others maintained by me. MISC TO BE PLACED: Post 455365 (Bwiti: "Novel Phenylcyclohexylamines..", Methods Discourse) Post 424992 (Bwiti: "1-(1-Phenylcyclohexyl)-4-phenylpiperidine", Methods Discourse) Patents: contributed by Cyrax in: Post 356567 (Cyrax: "PCP Patents, a compendium", Methods Discourse) Patent GB836083 Patent GB837747 Patent US2921076 Patent US3097136 Patent US3145229 Patent US5248686 Contributed by Bwiti in: Post 357544 (Bwiti: "That's good news!", Methods Discourse) Patent GB758143 Patent GB838748 Patent GB853775 Patent GB861350 Patent US3192219 Patent US3097207 Patent GB836083 Patent GB837747 Patent US5969159 Patent US3097136 Patent US3145229 Patent US3097136 Patent US3247200 Patent US3522273 Patent US2921076 Patent US3254124 References Requested Specifically for this Digest: Post 361229 (Bwiti: "Needed References", Methods Discourse) (before sending of these refs- be sure that they haven't already been posted here or in posts subsequent to 361229 in that same thread) Post 361271 (Rhodium: "More PCP", Methods Discourse) Post 378784 (Rhodium: "Rigid PCP Analogs - Binding to Sigma/PCP receptors", Methods Discourse) Mostly Pharm info, but some synth: Post 507205 (7is: "More PCP related studies", Methods Discourse) -- be sure to check the following threads also. Precursors Cyclohexanone by ox. of Cyclohexanol with KMnO₄ Post 285993 (Elementary: "Oxidation of cyclohexanol with KMnO4", Methods Discourse) 1,5-Dibromopentane: Post 436097 (pHarmacist: "1,5-dibromopentane", Methods Discourse) Post 288137 (Antoncho: "A cool PCP synthesis", Novel Discourse) Post 184706 (Rhodium: "Re: Help to make 1,5-dibromopentane (Method). for PCP", Novel Discourse) PCA: Post 105162 (Slappy: "PCA question", Chemistry Discourse) PCC: 1-Piperidinyl Cyclohexanecarbonitrile (& analogues) Post 172690 (slappy: "Re: Weight of PCC-Analogue(from methylamine).....", Chemistry Discourse) Post 101408 (Beagle: "Question about 1-piperidine-carbonitrile...", Chemistry Discourse) -- Post 465740 (josef_k: "phenylcyclopentylketone", Novel Discourse) Post 465792 (Manichi: "Cyclohexene -persulfate/CuSO4->CyclopentaneCOOH", Novel Discourse) Post 466155 (Vitus_Verdegast: "Great work Manichi!!", Novel Discourse) Act quickly or not at all.