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All 3 posts   Subject: rxtalization of 2-(chloroacetamido)-5-chlorobenzop   Please login to post   Down

(Hive Bee)
09-17-04 13:06
No 531772
      rxtalization of 2-(chloroacetamido)-5-chlorobenzop     

Hi there,

anyone know what an appropriate rextalization solvent for 2-(chloroacetamido)-5-chlorobenzophenone might be?

many thanks.
(Hive Addict)
09-18-04 21:29
No 532036
User Picture 
      About your material in question....     

Maybe by checking out this article , you can find your

One-Pot Synthesis of 2-(N-Methyl-2-chloroacetamido)-5-chlorobenzophenone


it may be archived here.....

I found the reference here using a korean search engine.....

It is better to die on your feet than to live on your knees...Emiliano Zapata
(Chief Bee)
09-19-04 01:02
No 532068
User Picture 
      Lit. mp.     

Melting Points (with recrystallization solvent and Literature reference) for CAS [4016-85-7]

119-121°C (ethanol) J.Org.Chem. 27, 562 (1962)
117-118°C (benzene, petroleum ether) J.Org.Chem. 27, 3781 (1962)
117-118°C (benzene, diethyl ether, petroleum ether) Patent DE1136709 (Chem.Abstr. 59, 12827, 1963)

The Hive - Clandestine Chemists Without Borders

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