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All 3 posts Subject: rxtalization of 2-(chloroacetamido)-5-chlorobenzop Please login to post Down

starlight
(Hive Bee)
09-17-04 13:06
No 531772
      rxtalization of 2-(chloroacetamido)-5-chlorobenzop

Hi there,

anyone know what an appropriate rextalization solvent for 2-(chloroacetamido)-5-chlorobenzophenone might be?

many thanks.

java
(Hive Addict)
09-18-04 21:29
No 532036
User Picture       About your material in question....

Maybe by checking out this article , you can find your answer.......java

One-Pot Synthesis of 2-(N-Methyl-2-chloroacetamido)-5-chlorobenzophenone

CHINESE JOURNAL OF PHARMACEUTICALS, 26, 49,1995

it may be archived here.....http://zgyygy.periodicals.net.cn/default.html

I found the reference here using a korean search engine.....

http://science.empas.com/search/kisti_detail.html?sn=20051743033

It is better to die on your feet than to live on your knees...Emiliano Zapata

Rhodium
(Chief Bee)
09-19-04 01:02
No 532068
User Picture       Lit. mp.

Melting Points (with recrystallization solvent and Literature reference) for CAS [4016-85-7]

119-121°C (ethanol) J.Org.Chem. 27, 562 (1962)
117-118°C (benzene, petroleum ether) J.Org.Chem. 27, 3781 (1962)
117-118°C (benzene, diethyl ether, petroleum ether) Patent DE1136709 (Chem.Abstr. 59, 12827, 1963)

^{The Hive - Clandestine Chemists Without Borders}

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	All 3 posts		Subject: rxtalization of 2-(chloroacetamido)-5-chlorobenzop		Please login to post		Down


		starlight (Hive Bee) 09-17-04 13:06 No 531772				rxtalization of 2-(chloroacetamido)-5-chlorobenzop
						Hi there, anyone know what an appropriate rextalization solvent for 2-(chloroacetamido)-5-chlorobenzophenone might be? many thanks.



		java (Hive Addict) 09-18-04 21:29 No 532036				About your material in question....
						Maybe by checking out this article , you can find your answer.......java One-Pot Synthesis of 2-(N-Methyl-2-chloroacetamido)-5-chlorobenzophenone CHINESE JOURNAL OF PHARMACEUTICALS, 26, 49,1995 it may be archived here.....http://zgyygy.periodicals.net.cn/default.html I found the reference here using a korean search engine..... http://science.empas.com/search/kisti_detail.html?sn=20051743033 It is better to die on your feet than to live on your knees...Emiliano Zapata



		Rhodium (Chief Bee) 09-19-04 01:02 No 532068				Lit. mp.
						Melting Points (with recrystallization solvent and Literature reference) for CAS [4016-85-7] 119-121°C (ethanol) J.Org.Chem. 27, 562 (1962) 117-118°C (benzene, petroleum ether) J.Org.Chem. 27, 3781 (1962) 117-118°C (benzene, diethyl ether, petroleum ether) Patent DE1136709 (Chem.Abstr. 59, 12827, 1963) ^{The Hive - Clandestine Chemists Without Borders}

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