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All 3 posts   Subject: rxtalization of 2-(chloroacetamido)-5-chlorobenzop   Please login to post   Down

 
    starlight
(Hive Bee)
09-17-04 13:06
No 531772
      rxtalization of 2-(chloroacetamido)-5-chlorobenzop     

Hi there,

anyone know what an appropriate rextalization solvent for 2-(chloroacetamido)-5-chlorobenzophenone might be?

many thanks.
 
 
 
 
    java
(Hive Addict)
09-18-04 21:29
No 532036
User Picture 
      About your material in question....     

Maybe by checking out this article , you can find your answer.......java

One-Pot Synthesis of 2-(N-Methyl-2-chloroacetamido)-5-chlorobenzophenone

CHINESE JOURNAL OF PHARMACEUTICALS, 26, 49,1995


it may be archived here.....http://zgyygy.periodicals.net.cn/default.html

I found the reference here using a korean search engine.....

http://science.empas.com/search/kisti_detail.html?sn=20051743033

It is better to die on your feet than to live on your knees...Emiliano Zapata
 
 
 
 
    Rhodium
(Chief Bee)
09-19-04 01:02
No 532068
User Picture 
      Lit. mp.     

Melting Points (with recrystallization solvent and Literature reference) for CAS [4016-85-7]

119-121°C (ethanol) J.Org.Chem. 27, 562 (1962)
117-118°C (benzene, petroleum ether) J.Org.Chem. 27, 3781 (1962)
117-118°C (benzene, diethyl ether, petroleum ether) Patent DE1136709 (Chem.Abstr. 59, 12827, 1963)

The Hive - Clandestine Chemists Without Borders
 
 

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